| Download | - View final version: A method for the identification of the mono-O-methylglucoses (PDF, 391 KiB)
|
|---|
| DOI | Resolve DOI: https://doi.org/10.1139/v53-110 |
|---|
| Author | Search for: Lemieux, R. U.1; Search for: Bauer, H. F.1 |
|---|
| Affiliation | - National Research Council of Canada. Prairie Regional Laboratory
|
|---|
| Format | Text, Article |
|---|
| Abstract | Periodate oxidation of any one mono-O-methylglucopyranose and alkaline hydrolysis of the product yields a substance which can be positively distinguished by paper chromatography from the products formed under the same conditions from the other mono-O-methylglucopyranoses. Thus, the components of a mixture of the mono-O-methylglucopyranoses can be readily identified. The method appears useful for the identification of di-O-methylglucoses. Reduction with sodium borohydride prior to periodate oxidation renders the method useful for the identification of tri-O-methylglucoses. The potential value of the method, which can be used on a microscale, is illustrated by an application to the characterization of the O-methylglucoses derived from a water-soluble O-methyl-cellulose |
|---|
| Publication date | 1953-09-01 |
|---|
| Publisher | Canadian Science Publishing |
|---|
| In | |
|---|
| Language | English |
|---|
| Peer reviewed | Yes |
|---|
| NRC number | NRCC 3044 |
|---|
| Export citation | Export as RIS |
|---|
| Report a correction | Report a correction (opens in a new tab) |
|---|
| Record identifier | 6be3eb69-267d-4ae1-9826-01b73e861757 |
|---|
| Record created | 2023-09-14 |
|---|
| Record modified | 2024-05-03 |
|---|